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For example, one guideline suggests trying ~1030% acetic acid in water for a stubborn basic peptide, or a few microliters of 1 N NaOH for an acidic peptide, then diluting to the required volume4

Pang et al., 2021

If you want to make ice as quickly as possible, lower the temperature of your freezer, and try freezing bottled or purified water instead of tap water